WebThe percent yield was calculated to be 64%. The final product of the experiment was pure Triphenylmethanol. The melting point obtained using the MEL-TEMP apparatus was 159°C. The literature melting point of the Triphenylmethanol is 162°C. The melting point was a way of determining the purity of the product. Web11 okt. 2013 · The literature melting point of Triphenylmethanol is 161.5째C. The IR had contained all of the expected pecks which were Csp2-H, C=C, and O-H.
Triphenylmethanol Lab - Preparation of Grignard Reagent
WitrynaTo help you get started, we’ve selected a few reselect examples, based on popular ways it is used in public projects. Secure your code as it's written. Use Snyk Code to scan source code in minutes - no build needed - and fix issues immediately. Web23 nov. 2011 · Melting point of triphenylmethanol = 153°C ~ 156°C Discussion: The purpose of this experiment is to synthesis triphenylmethanol by using Grignard reagent. In order to synthesis triphenylmethanol, Grignard reagent is playing an important role because Grignard reagent is the key reagent in this experiment. cteasy tarn et garonne
theoretical yield of triphenylmethanol - afnw.com
WebDiscuss if and when melting points can be used to determine the purity of organic and inorganic compounds and if and when melting points can be used to identify organic and inorganic compounds. Explain how some solids (compounds that are solids at room temperature) can be analyzed by gas chromatography. WebLiterature melting point of triphenylmethanol = 164 C Literature melting point of 1,2,4,5-tetrachlorobenzene = 140 C Calculation : Benzoic acid : Filter paper: 1+2 = 0.3372g + 0.3251g = 0.6623g Watch glass: 18.3829g + 19.2723g = 37.6552 Extraction NaOH (after drying) = 38.4235g – 38.3176g = 0.1059g 𝑅𝑒𝑐𝑜𝑣𝑒𝑟𝑒𝑑 𝑤𝑒𝑖𝑔ℎ𝑡 WebFor this lab, certain actions were performed to facilitate the optimize conditions in and Grignard reaction to proceed. As mentioned above, forming the Grignard agent and the Grignard reaction must take place in dry, absolute conditions. earth books for kindergarten